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The third method uses an alcohol such as sec-butanol as the acid, and since it will protonate only the organometallic, no correction for hydroxide is necessary The other key to this method is the indicator, phenanthroline or bipyridyl These have the property that they form colored complexes with lithium and magnesium reagents In their presence, a brown color is usually observed In their absence, a yellow or clear solution is seen The titration is performed with an automatic burette (Fig 26) under an inert atmosphere The automatic burette has a lower reservoir that can be lled with titrant (ca 06 m sec-butanol in anhydrous xylene, determined volumetrically) The section of the burette that we would recognize as a burette is lled with titrant by pumping a rubber bulb and forcing liquid up into the burette with pressure.

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tence of impairment indicators are based on market conditions and operational performance. Future events could cause management to conclude that impairment indicators exist and that the value of long-lived assets and goodwill associated with acquired businesses is impaired. Goodwill is evaluated for impairment annually under the provisions of FAS 142 which requires us to make judgments relating to future cash flows and growth rates as well as economic and market conditions. Revenue Recognition We recognize sales revenue at the time a sale is made to the customer, except for the following types of transactions. Layaway transactions are recognized when the customer satisfies all payment obligations and takes possession of the merchandise. We recognize SAM S CLUB membership fee revenue over the 12-month term of the membership. Customer purchases of Wal-Mart/SAM S CLUB shopping cards are not recognized until the card is redeemed and the customer purchases merchandise using the shopping card. Defective merchandise returned by customers is either returned to the supplier or is destroyed and reimbursement is sought from the supplier. Insurance/Self-Insurance We use a combination of insurance, self-insured retention, and/or self-insurance for a number of risks including workers compensation, general liability, vehicle liability and employee-related health care benefits, a portion of which is paid by the Associates. Liabilities associated with the risks that we retain are estimated in part by considering historical claims experience, demographic factors, severity factors and other actuarial assumptions. The estimated accruals for these liabilities could be significantly affected if future occurrences and claims differ from these assumptions and historical trends. For a complete listing of our accounting policies, please see Note 1 to our consolidated financial statements that appear after this discussion.

It is a convenient apparatus to store and maintain the titrant solution and encourages frequent titration Anhydrous tetrahydrofuran (ca 3 mL) and the indicator (20 mg) are added to a round-bottom ask with a stir bar A known amount of organometallic is added, and the color should develop Titrant is added from the automatic burette until the color is just discharged Provided that the endpoint is not greatly exceeded, replicate titrations can be performed in the same ask to obtain a more precise value It is also certainly possible to prepare solutions of reagents oneself A particular instance where this may be useful and for which commercial sources are often not available is volatile compounds A classic example is anhydrous HCl in methanol.

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are generally within or slightly above the normal range (Thomas & Douglas 2001) LVH is concentric, more pronounced, and occurs secondary to the pressure load in strength-trained athletes, whereas in endurance athletes it is eccentric and occurs as an adaptation to the increased cavity dimensions in order to maintain normal wall stress Left ventricular wall thickness >12 mm is unusual and rarely exceeds 16 mm even in the most elite athletes (Pelliccia et al 1991; Thomas & Douglas 2001) Values above this rage should raise the possibility of hypertrophic cardiomyopathy Noteworthy, LVH above the normal range is generally not observed in female athletes (Pelliccia et al 1991) The calculated left ventricular mass is also 45 50% greater in well-trained athletes compared to sedentary controls (Thomas & Douglas 2001).

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